Ukubuka: 115 Umbhali: Isikhathi Sokushicilela Isihleli Sesayithi: 2024-05-17 Umsuka: Isayithi
I-Polymer APS idlala indima ebalulekile embonini yesimanje, futhi izakhiwo zayo ezisebenzayo ziyenza isetshenziswe kabanzi emikhakheni ehlukahlukene. I-APS ayibonisi nje ukumelana nesimo sezulu esihle kakhulu nokuzinza kwamakhemikhali, kodwa futhi ikhombisa izakhiwo ezinhle kakhulu zemishini nezikagesi, okuyenza ibe ukukhetha okuhle kwezinto eziningi. Phakathi kwazo, ijeli ye-APS, njengokuphuma kwe-APS, ibonise inani eliyingqayizivele lesicelo emikhakheni eminingi.
Kulo mongo, lesi sihloko sizoxoxa ngokubaluleka kokwenza ijeli ye-APS engu-10%. Ngokutadisha inqubo yokulungiselela kanye nezakhiwo zejeli ye-APS ngokuningiliziwe, singaqonda ngokujulile amandla kanye nezinzuzo zale nto ekusetshenzisweni okungokoqobo. Ezinhlelweni eziningi, ukulungiswa kwejeli ye-APS engu-10% akugcini nje ukudlala indima ebalulekile ekuthuthukiseni ukusebenza kwe-APS, kodwa futhi kunokubaluleka okubalulekile okusebenzayo emikhakheni yezinto ze-elekthronikhi, okokumboza, amadivaysi ezokwelapha, njll.
Ngakho-ke, ngokuxoxa ngokubaluleka kokulungiswa kwejeli ye-APS engu-10%, singaqonda kangcono amathemba okusetshenziswa kwezinto ze-APS, futhi sinikeze ukukhanyiselwa okuwusizo kocwaningo nokuthuthukiswa kwezimboni emikhakheni ehlobene.
Igama eliphelele le-APS yi-Acrylonitrile Butadiene Styrene Copolymer. I-APS iyimpahla ye-polymer enesakhiwo se-molecular ehlanganisa ama-monomers amathathu: i-butyl acrylate, i-benzyl acrylate, ne-propylene acrylate. Le copolymer inezinto eziningi ezinhle kakhulu, okwenza isetshenziswe kabanzi emikhakheni ehlukene.
Imisebenzi ye-APS ibonakala kakhulu ekumelaneni kwayo nesimo sezulu, ukuqina kwamakhemikhali, izakhiwo zemishini nezikagesi. Inokumelana nesimo sezulu esihle kakhulu futhi ingagcina uzinzo ezindaweni ezinokhahlo, iyenze ibe yinhle kakhulu ezindaweni ezingaphandle nezinezinga eliphezulu lokushisa. Ngaleso sikhathi, i-APS iphinde ikhombise ukuzinza okuphezulu kwamakhemikhali nokumelana okuhle nezinto eziningi zamakhemikhali. Mayelana nokusebenza kwemishini, i-APS inamandla amakhulu nokuqina, okwenza idume kakhulu ekukhiqizeni amapulasitiki obunjiniyela ahlukahlukene kanye nemikhiqizo ehlala isikhathi eside. Ngaphezu kwalokho, i-APS iphinde ibe nokusebenza kahle kukagesi futhi ilungele izinkambu ze-elekthronikhi nezinto zikagesi.
Kujeli, indima ye-APS ibonakala ngokulungiselela ijeli ye-APS. Ijeli ye-APS ivamise ukwakhiwa ngokuxuba i-APS ne-solvent efanele noma ingxube kanye ne-polymerizing ngaphansi kwezimo ezithile. Ijeli ye-APS idlala indima ebalulekile ekucutshungulweni nasekusetshenzisweni kwezinto ezibonakalayo, ihlinzeka ngefomu lezinto ezibonakalayo elinepulasitiki elihle kanye nokubumba okulula. I-APS efomini yejeli isetshenziswa kakhulu ekubanjeni, emikhiqizweni yepulasitiki, emishinini yezokwelapha nakwezinye izinkambu, ihlinzeka ngezinhlobonhlobo zokusebenza nezici zokusetshenziswa kwemikhiqizo kule mikhakha.
I-Polymer APS idlala indima ebalulekile embonini yesimanje, futhi izakhiwo zayo ezisebenzayo ziyenza isetshenziswe kabanzi emikhakheni ehlukahlukene. I-APS ayibonisi nje ukumelana nesimo sezulu esihle kakhulu nokuzinza kwamakhemikhali, kodwa futhi ikhombisa izakhiwo ezinhle kakhulu zemishini nezikagesi, okuyenza ibe ukukhetha okuhle kwezinto eziningi. Phakathi kwazo, ijeli ye-APS, njengokuphuma kwe-APS, ibonise inani eliyingqayizivele lesicelo emikhakheni eminingi.
Kulo mongo, lesi sihloko sizoxoxa ngokubaluleka kokwenza ijeli ye-APS engu-10%. Ngokutadisha inqubo yokulungiselela kanye nezakhiwo zejeli ye-APS ngokuningiliziwe, singaqonda ngokujulile amandla kanye nezinzuzo zale nto ekusetshenzisweni okungokoqobo. Ezinhlelweni eziningi, ukulungiswa kwejeli ye-APS engu-10% akugcini nje ukudlala indima ebalulekile ekuthuthukiseni ukusebenza kwe-APS, kodwa futhi kunokubaluleka okubalulekile okusebenzayo emikhakheni yezinto ze-elekthronikhi, okokumboza, amadivaysi ezokwelapha, njll.
Ngakho-ke, ngokuxoxa ngokubaluleka kokulungiswa kwejeli ye-APS engu-10%, singaqonda kangcono amathemba okusetshenziswa kwezinto ze-APS, futhi sinikeze ukukhanyiselwa okuwusizo kocwaningo nokuthuthukiswa kwezimboni emikhakheni ehlobene.
Igama eliphelele le-APS yi-Acrylonitrile Butadiene Styrene Copolymer. I-APS iyimpahla ye-polymer enesakhiwo se-molecular ehlanganisa ama-monomers amathathu: i-butyl acrylate, i-benzyl acrylate, ne-propylene acrylate. Le copolymer inezinto eziningi ezinhle kakhulu, okwenza isetshenziswe kabanzi emikhakheni ehlukene.
Imisebenzi ye-APS ibonakala kakhulu ekumelaneni nesimo sezulu, ukuqina kwamakhemikhali, izakhiwo zemishini nezikagesi. Inokumelana nesimo sezulu esihle kakhulu futhi ingagcina uzinzo ezindaweni ezinokhahlo, iyenze ibe yinhle kakhulu ezindaweni ezingaphandle nezinezinga eliphezulu lokushisa. Ngaleso sikhathi, i-APS iphinde ikhombise ukuzinza okuphezulu kwamakhemikhali nokumelana okuhle nezinto eziningi zamakhemikhali. Mayelana nokusebenza kwemishini, i-APS inamandla amakhulu nokuqina, okwenza idume kakhulu ekukhiqizeni amapulasitiki obunjiniyela ahlukahlukene kanye nemikhiqizo ehlala isikhathi eside. Ngaphezu kwalokho, i-APS iphinde ibe nokusebenza kahle kukagesi futhi ilungele izinkambu ze-elekthronikhi nezinto zikagesi.
Kujeli, indima ye-APS ibonakala ngokulungiselela ijeli ye-APS. Ijeli ye-APS ivamise ukwakhiwa ngokuxuba i-APS ne-solvent efanele noma ingxube kanye ne-polymerizing ngaphansi kwezimo ezithile. Ijeli ye-APS idlala indima ebalulekile ekucutshungulweni nasekusetshenzisweni kwezinto ezibonakalayo, ihlinzeka ngefomu lezinto ezibonakalayo elinepulasitiki elihle kanye nokubumba okulula. I-APS efomini yejeli isetshenziswa kakhulu ekubanjeni, emikhiqizweni yepulasitiki, emishinini yezokwelapha nakwezinye izinkambu, ihlinzeka ngezinhlobonhlobo zokusebenza nezici zokusetshenziswa kwemikhiqizo kule mikhakha.
Ukulungisa indawo yaselabhorethri kuyisinyathelo esibalulekile ekuqinisekiseni ukunemba nokuphepha kocwaningo.
Sebenzisa i-ejenti yokuhlanza efanelekile, njengesixazululo se-ethanol esingu-75%, ukuze usule itafula lokuhlola ukuze uqinisekise indawo ehlanzekile.
Hlanza njalo futhi ubulale amathuluzi aselabhorethri, njengama-test tube racks, izinto ezilungiswayo, ama-pipette, njll. Sebenzisa utshwala noma ezinye izibulala-magciwane ezifanele.
Naka ukuhlanza izingxenye zangaphakathi zemishini yaselabhorethri, njenge-centrifuge turntable kanye nengaphakathi le-incubator.
Hlela futhi ulahle imfucuza kanye nemfucuza yaselabhorethri emigqonyeni ehambisanayo ukuze kuqinisekiswe ukulahlwa kahle kwemfucuza.
Hlala uthulula udoti waselabhorethri ukuze ugweme ukunqwabelana kwamagciwane abulalayo noma amakhemikhali ayingozi.
Qinisekisa ukusebenza kahle kwesistimu yokungenisa umoya yaselabhorethri, buyisela umoya ngesikhathi, futhi unciphise ukugcwala kwamagesi ayingozi.
Hlanza njalo izintuba zokungenisa umoya zaselabhorethri kanye nezihlungi zesimo somoya ukuze uqinisekise ukuhamba komoya okubushelelezi.
Izisebenzi zokuhlola kufanele zigcine inhlanzeko yomuntu siqu, okuhlanganisa ukugeza izandla, ukugqoka izingubo zaselabhorethri, nezinto zokuzivikela.
Ngaphambi nangemuva kokungena elabhorethri, hlanza kahle izandla ngesibulali magciwane sesandla noma ngesibulali magciwane sesandla.
Gcina futhi ulinganise imishini yaselabhorethri njalo ukuze uqinisekise ukusebenza kwayo okuvamile.
Uma kukhona noma yimuphi umonakalo noma okokusebenza okudinga ukulungiswa, yazisa ngokushesha izisebenzi ezifanele ukuze zisingathwe.
Hlanza imiphetho yelabhorethri, okuhlanganisa indawo yokungena namaphasishi, ukuze ugweme ukunqwabelana kwemfucumfucu.
Ngesikhathi sokuhlolwa, landela ngokuqinile izinqubo zokusebenza zokuphepha futhi usebenzise izinto zokuzivikela ngendlela efanele, njengamagilavu okuhlola, izibuko, njll.
Izinto ezidingekayo ziyisinyathelo esibalulekile sokuqinisekisa ukuqhubeka kahle kokuhlolwa.
I-butyl acrylate
I-Butadiene
I-styrene
Izincibilikisi (njenge-toluene noma i-xylene)
I-ejenti yokuqala (isb. ammonium persulfate)
I-Crosslinking agent (isb. i-diethyleneformamide)
Qinisekisa ukuthi izinto zokusetshenziswa ezikhethiwe zisezingeni eliphezulu nobumsulwa, ngoba kuthinta ngqo ukusebenza kwejeli nemiphumela yokuhlola. Ukusetshenziswa kwezinto zokusetshenziswa ezinekhwalithi ephansi noma ukungcola okuphezulu kungaholela ekusebenzeni kwejeli okungazinzile futhi kuthinte ukunemba kokuhlolwa.
Gqoka amagilavu aselabhorethri kanye nezibuko: Ngaphambi kokwenza noma yimiphi imisebenzi yokuhlola, qiniseka ukuthi ugqoka amagilavu nezibuko ezihlangabezana nezindinganiso zokuphepha zaselabhorethri ukuze uvikele isikhumba namehlo ezintweni eziyingozi.
Ukungenisa komoya endaweni yaselabhorethri: Lapho wenza noma yimiphi imisebenzi ehilela izinyibilikisi zemvelo noma amagesi ayingozi, qinisekisa ukuthi uhlelo lokungenisa umoya laselabhorethri lusebenza kahle ukuze unciphise ukugcwala kwezinto eziyingozi.
Isisindo sezinto ezibonakalayo: sebenzisa ibhalansi enembile ukuze ukale ngokunembile izinto zokusetshenziswa ukuze uqinisekise ingxenye enembile yengxenye ngayinye ekuhlolweni, ukuze uthole ukusebenza kwejeli okungaguquki.
Izindlela zokuphepha zokusebenzisa izincibilikisi: Uma usebenzisa izincibilikisi zemvelo, qiniseka ukuthi usebenza endaweni enomoya omuhle ukuze ugweme ukulimala komhwamuko wazo empilweni.
Gwema amalangabi avulekile nemithombo yokushisa ukuze uvimbele imililo ebangelwa yizincibilikisi.
Ukwengezwa kwabaqalisi nama-ejenti axhumanisayo: Uma wengeza abaqalisi nama-ejenti axhumanisayo, kufanele kuqashelwe ukuze kuqinisekiswe ukusebenza okunembile futhi kuvinjwe imiphumela eyeqisayo noma enganele ekuhlolweni.
Ngemuva kokuhlolwa, lahla imfucuza ngendlela efanele bese uyihlukanisa futhi uyilahle ngokwemithetho yelabhorethri.
Gqoka amagilavu aselabhorethri kanye nezibuko ukuze uqinisekise ukungena komoya okuhle elabhorethri.
Lungiselela izinto zokuhlola ezidingekayo, okuhlanganisa izikali, iziqukathi, izinduku ezinyakazayo, njll.
Usebenzisa ibhalansi enembile, kala ngokunembile amamonomeri e-copolymer adingekayo njenge-butyl acrylate, i-benzyl acrylate, ne-acrylic acid ester ngokuya ngefomula yokuhlola.
Qinisekisa ukuthi ukulinganisa kwengxenye ngayinye kunembile ukuze kugcinwe ukusebenza okulindelekile kwejeli.
Faka ama-monomers alinganisiwe njenge-butyl acrylate, i-benzyl acrylate, ne-propylene acrylate esitsheni sokuxuba.
Engeza inani elifanele le-solvent (njenge-toluene noma i-xylene) ukuze uvumele ama-monomers ukuthi axubane ngokulinganayo.
Sebenzisa induku eshukumisayo ukuze ugovuze futhi uqinisekise ukuthi ingxube ifana, yakha ingxube ye-homogeneous liquid.
Engeza inani elifanele lesiqalisi engxubeni bese ugovuze ngokulinganayo ukuze uqalise ukusabela kwe-polymerization.
Engeza i-ejenti yokuxhumanisa ukuze uqinisekise ukwakheka kwesakhiwo senethiwekhi esinezinhlangothi ezintathu, ukuze ijeli ibe namandla adingekayo nokuzinza.
Beka ingxube ngaphansi kwezimo ezifanele zokushisa ukuze ukhuthaze ukusabela kwe-polymerization kwama-monomers aqalwe ngumqalisi.
Lawula isikhathi sokuphendula ukuze uqinisekise ukuthi ukusabela kwe-polymerization kwenziwa ngokugcwele ukwakha isakhiwo sejeli.
Ngokuqhubeka kwe-polymerization, ingxube kancane kancane ishintsha ibe yi-gel state. Lawula isikhathi sokusabela kanye nezinga lokushisa ukuze uqinisekise ukufana kanye nekhwalithi yokwakheka kwejeli.
Ijeli eyakhiwe kufanele iphathwe kahle, njengokusika, ukubumba noma ukwelashwa okwengeziwe, ukuhlangabezana nezidingo zangempela zokufaka isicelo.
Hlanza amathuluzi okuhlola futhi uhlukanise imfucuza ngokwemithetho yaselabhorethri.
Ukwengeza i-APS engu-10% kuyisinyathelo esibalulekile sokwakha isakhiwo senethiwekhi yejeli. Ukwengezwa kwe-APS kuthinta ngqo amandla, ukuzinza kanye nezinye izakhiwo zejeli.
Ukwengezwa okulungile kwe-10% APS kungathuthukisa ukuqina, ukuqina kwamakhemikhali namandla emishini yejeli, okubalulekile ekuhlolweni nasekusetshenzisweni.
Lungiselela inani elifanele le-10% APS (butyl acrylate benzyl methacrylate acrylic ester copolymer) isisombululo. Qinisekisa ukugxila okunembile kwe-10% APS ukuze uhlangabezane nezidingo zokuhlola.
Ngesikhathi esifanele se-polymerization, kancane kancane engeza isixazululo se-APS esingu-10% esilungisiwe kungxube yejeli eyakhiwayo.
Qinisekisa ukunyakaziswa okufanayo futhi ugweme ukweqisa kwendawo noma isisombululo se-APS esingu-10% esinganele.
Ngokwezidingo zokuhlola kanye nenani elingeziwe elingu-10% APS, kungase kudingeke ukuthi ulungise izinga lokushisa nesikhathi sokusabela ukuze uqinisekise ukuthi u-10% we-APS ubamba iqhaza ngokugcwele ku-polymerization futhi yakhe isakhiwo sejeli esifanayo.
Ngemuva kokungeza i-10% APS, qhubeka ugoqa futhi uxube ukuze uqinisekise ukuthi zonke izithako zengxube yejeli zisakazwa ngokulinganayo ukuze uthole ikhwalithi yejeli engaguquki.
Ngokusho komklamo wokuhlola, qeda ukusabela kwe-polymerization ngesikhathi esifanele. Lokhu kungafinyelelwa ngokungeza izinqamuli zokusabela ezifanele noma ukulungisa izimo zokusabela.
Ngokuqhubekayo uqaphe inqubo yokwakheka kwejeli ukuze uqinisekise ukuthi ukungezwa kwe-10% APS kuthuthukisa ukusebenza kwejeli.
Ngemva kokwakhiwa kwejeli, ukwelashwa okufanele okulandelayo, njengokuhlanza, ukusika noma ukubunjwa, kuzokwenziwa ukuze kuhlangabezane nezidingo zangempela zohlelo lokusebenza.
Izakhiwo zomzimba nezamakhemikhali zejeli zingashintshwa ngokulungisa isilinganiso se-butyl acrylate, i-benzyl acrylate ne-acrylic ester. Ngokulungiselela ngokucophelela isilinganiso se-monomer, singathola izakhiwo zejeli ezihambisana kakhulu nezidingo zangempela.
Ngokwenhloso yokuhlola kanye nezici zejeli ezidingekayo, lungisa inani kanye nohlobo lwesiqalisi kanye ne-crosslinker. Isiqalisi esifanelekile kanye ne-ejenti yokuxhumanisa kungathinta amandla, ukunwebeka nokuzinza kwejeli.
Ukulungisa izinga lokushisa kanye nesikhathi se-polymerization kungathinta isivinini se-polymerization kanye nezinga lejeli. Ngokulawula ngokucophelela lezi zici ezimbili, ijeli esebenza kangcono ingatholakala.
Ukwethulwa kwamanye ama-modifiers, njengama-surfactants noma ama-plasticizers, kungalungisa izakhiwo ezingaphezulu nokucutshungulwa kwejeli. Lokhu kuwusizo kakhulu ekuguquleni ijeli ezimeni ezithile zohlelo lokusebenza.
Cabangela ukukhetha isinyibilikisi esifaneleka kakhulu ukuze uqinisekise ukuthi ama-monomers angahlakazwa ngokufanayo futhi enziwe i-polymerized kangcono. Izinyibilikisi ezihlukene zinethonya elikhulu ekwakhekeni nasezimpahleni zejeli.
Sebenzisa amathuluzi okulinganisa anembile kanye nemishini ezenzakalelayo ukuze uqinisekise ukuthi inani lesithako ngasinye esingezwe linembile ukuze kugcinwe ukuvumelana kwejeli.
Hlala ulungisa futhi ulungiselele izimo phakathi nokuhlolwa, futhi impendulo ingenziwa ngokuya ngemiphumela yokuhlola ukuthuthukisa kancane kancane ukusebenza kwejeli.
Amasu okuhlaziya athuthukile njengokuskena i-electron microscope (SEM) kanye ne-nuclear magnetic resonance (NMR) asetshenziselwa ukuhlaziya i-microstructure yejeli ngokuningiliziwe ukuze kuqondwe kangcono kanye nokuthuthukisa izici zejeli.
Ngaphambi kokwenza noma yimiphi imisebenzi yokuhlola, qiniseka ukuthi ugqoka amagilavu aselabhorethri kanye nezibuko ukuze uvikele isikhumba namehlo ezintweni eziyingozi.
Sebenza endaweni enomoya omuhle elabhorethri ukunciphisa ukugcwala komhwamuko we-organic solvent namanye amagesi ayingozi.
Sebenzisa izinto zokuzivikela ezifanele njengezimpahla ezivikela amakhemikhali, ikakhulukazi lapho uphatha izinto eziyingozi.
Qinisekisa ukusetshenziswa kwempahla yokuhlola efanele, ehlanzekile, nengalimele, ikakhulukazi ama-rod anyakazayo, iziqukathi, namasilinda okulinganisa.
Naka ukulinganisa nokugcinwa kwemishini yaselabhorethri ukuqinisekisa ukusebenza kwayo okuvamile.
Gwema ukuthintana okuqondile kwesikhumba nezinto eziyingozi, ikakhulukazi izincibilikisi zemvelo nama-polymer precursors. Uma uthintana, hlambulula ngokushesha indawo ethintekile ngamanzi amaningi.
Gwema amalangabi avulekile nemithombo yokushisa, ikakhulukazi uma usebenzisa izincibilikisi ezivuthayo nezinhlanganisela eziphilayo.
Misa izinto zokucisha umlilo elabhorethri futhi uqonde izindlela ezifanele zokuzisebenzisa.
Qinisekisa ukulawula okunembile kwezinga lokushisa lokusabela, isikhathi kanye nengcindezi ukuze ugweme ukusabela okungalindelekile kanye nejeli ingalawuleki.
Sebenzisa amathuluzi okuhlola ahlanzekile kanye nezindawo zokusebenza ukuze ugweme ukuhlanganisa izinto zokuhlola noma ukubangela ukungcola okuphambene.
Ngaphambi kokwenza ucwaningo, qonda izinqubo zokusabela ezimweni eziphuthumayo zaselabhorethri, okuhlanganisa izinombolo zocingo oluphuthumayo, izinto zosizo lokuqala, nezindawo zokuphuma eziphuthumayo.
Hlela futhi ulahle imfucuza ngokwemithetho yaselabhorethri ukuze ugweme ukungcoliswa kanye nobungozi bemvelo.
Bamba iqhaza ekuqeqeshweni okuvamile kokuphepha kwaselabhorethri ukuze uqonde amazinga akamuva okuphepha nezinqubo zokusebenza.
Ukulinganisa nokuxutshwa kwezinto ezingavuthiwe
Sebenzisa ibhalansi enembile ukuze ulinganise ama-copolymer monomers afana ne-butyl acrylate, i-benzyl acrylate, ne-propylene acrylate ukuze uqinisekise izilinganiso ezinembile.
Faka izinto ezingavuthiwe esitsheni sokuxuba, engeza i-solvent, bese ugoqa ngokulinganayo ukuze wenze ingxube yoketshezi efanayo.
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